Table 1. HPLC analysis conditions

Mobile phase A: water, B: acetonitrile
Flow rate 1 mL/min
Column Phenomenex Gemini 5 μm C18 110Å 250 × 4.6 nm
Column temperature 30°C
Wave length 254 nm
Runtime 10 min
Method Isocratic 80%(A) : 20%(B)